TA Instruments

AR1759-0001f

15/03/2013 16:20:07

Sample name	DI 40 mm AL P120
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1759
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 16:20:07

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	5.990	-45.059	10000	20.0	6.139	31.008	-14.69	7.488	-1.962	25010	5.2632	446.2	6.5790	657.90	3.411E-3	0.0	0.5
1.9960	9.769	12.407	10000	20.0	6.150	31.996	4.044	12.21	0.3312	25060	13.0973	168.0	16.372	1637.2	3.411E-3	0.0	0.5
3.0080	15.46	23.292	10000	20.0	6.150	33.008	7.592	19.32	0.3930	25060	26.8025	67.14	33.503	3350.3	3.411E-3	0.1	0.6
4.0080	18.40	30.765	10000	20.0	6.149	34.008	10.03	23.01	0.4359	25050	40.7643	47.34	50.955	5095.5	3.411E-3	0.1	0.6
5.0120	24.66	47.559	10000	20.0	6.146	35.012	15.50	30.82	0.5029	25040	67.4742	26.36	84.343	8434.3	3.411E-3	0.1	0.6
6.0080	31.57	69.878	10000	20.0	6.147	36.008	22.78	39.47	0.5771	25040	106.5990	16.08	133.25	13325	3.411E-3	0.1	0.6
6.9920	34.02	78.689	10000	20.0	6.147	36.992	25.65	42.52	0.6032	25040	126.2520	13.85	157.82	15782	3.411E-3	0.1	0.6
7.9960	39.29	97.797	10000	20.0	6.139	37.996	31.88	49.11	0.6491	25010	165.4660	10.37	206.83	20683	3.411E-3	0.1	0.6
9.0080	46.02	126.69	10000	20.0	6.136	39.008	41.29	57.52	0.7179	25000	223.1920	7.556	278.99	27899	3.411E-3	0.2	0.7
10.008	50.94	149.40	10000	20.0	6.133	40.008	48.70	63.67	0.7648	24990	274.5500	6.163	343.19	34319	3.411E-3	0.2	0.7
10.996	55.71	174.37	10000	20.0	6.127	40.996	56.83	69.63	0.8162	24960	325.8760	5.148	407.35	40735	3.411E-3	0.2	0.7
12.012	60.08	195.51	10000	20.0	6.122	42.012	63.73	75.11	0.8485	24950	377.2700	4.422	471.59	47159	3.411E-3	0.2	0.7
13.012	64.40	221.50	10000	20.0	6.116	43.012	72.20	80.50	0.8969	24920	434.5710	3.846	543.21	54321	3.411E-3	0.2	0.7
14.008	69.14	248.02	10000	20.0	6.117	44.008	80.84	86.42	0.9355	24920	498.4840	3.337	623.11	62311	3.411E-3	0.2	0.7
14.996	75.66	291.39	10000	20.0	6.103	44.996	94.98	94.58	1.004	24870	593.9550	2.780	742.44	74244	3.411E-3	0.2	0.7
16.012	79.91	318.42	10000	20.0	6.094	46.012	103.8	99.89	1.039	24830	664.1080	2.488	830.14	83014	3.411E-3	0.3	0.8
17.012	84.51	351.76	10000	20.0	6.092	47.012	114.7	105.6	1.085	24820	740.6080	2.224	925.76	92576	3.411E-3	0.3	0.8
18.016	90.97	398.96	10000	20.0	6.083	48.016	130.0	113.7	1.144	24790	856.7840	1.917	1071.0	1.0710E5	3.411E-3	0.3	0.8
19.000	95.02	429.43	10000	20.0	6.076	49.000	140.0	118.8	1.178	24760	930.9580	1.755	1163.7	1.1637E5	3.411E-3	0.3	0.8
20.008	99.38	462.99	10000	20.0	6.067	50.008	150.9	124.2	1.215	24720	1019.9000	1.602	1274.9	1.2749E5	3.411E-3	0.3	0.8
20.996	105.8	516.84	10000	20.0	6.060	50.996	168.5	132.3	1.274	24690	1153.3000	1.411	1441.6	1.4416E5	3.411E-3	0.3	0.8
22.024	109.9	557.03	10000	20.0	6.047	52.024	181.6	137.4	1.322	24640	1241.8500	1.306	1552.3	1.5523E5	3.411E-3	0.4	0.9
23.008	114.2	584.16	10000	20.0	6.040	53.008	190.4	142.8	1.334	24610	1343.3900	1.207	1679.2	1.6792E5	3.411E-3	0.4	0.9
24.000	120.6	652.44	10000	20.0	6.029	54.000	212.7	150.8	1.410	24560	1495.3800	1.080	1869.2	1.8692E5	3.411E-3	0.4	0.9
25.016	124.7	692.12	10000	20.0	6.017	55.016	225.6	155.9	1.447	24510	1596.7300	1.009	1995.9	1.9959E5	3.411E-3	0.4	0.9
26.008	129.0	736.21	10000	20.0	6.004	56.008	240.0	161.3	1.488	24460	1710.8000	0.9402	2138.5	2.1385E5	3.411E-3	0.4	0.9
27.004	135.4	805.61	10000	20.0	5.985	57.004	262.6	169.3	1.551	24390	1881.7600	0.8508	2352.2	2.3522E5	3.411E-3	0.5	1.0
28.008	139.6	848.47	10000	20.0	5.972	58.008	276.6	174.4	1.585	24330	1995.5601	0.7996	2494.5	2.4945E5	3.411E-3	0.5	1.0
29.008	143.6	913.83	10000	20.0	5.956	59.008	297.9	179.5	1.659	24270	2115.8601	0.7528	2644.8	2.6448E5	3.411E-3	0.5	1.0
30.008	150.0	995.82	10000	20.0	5.932	60.008	324.6	187.6	1.731	24170	2305.8301	0.6871	2882.3	2.8823E5	3.411E-3	0.5	1.0
31.012	154.1	1045.4	10000	20.0	5.922	61.012	340.8	192.7	1.768	24130	2432.8401	0.6499	3041.1	3.0411E5	3.411E-3	0.5	1.0
32.008	158.2	1105.3	10000	20.0	5.895	62.008	360.3	197.8	1.821	24020	2635.7000	0.6138	3294.6	3.2946E5	3.411E-3	0.5	1.0
33.008	164.7	1192.4	10000	20.0	5.880	63.008	388.6	205.8	1.888	23960	2773.9099	0.5656	3467.4	3.4674E5	3.411E-3	0.6	1.1
34.004	168.8	1251.1	10000	20.0	5.862	64.004	407.8	211.0	1.933	23880	2912.5901	0.5366	3640.7	3.6407E5	3.411E-3	0.6	1.1
35.008	174.9	1342.2	10000	20.0	5.835	65.008	437.5	218.6	2.001	23770	3127.3201	0.4976	3909.2	3.9092E5	3.411E-3	0.6	1.1
36.004	179.1	1403.3	10000	20.0	5.824	66.004	457.4	223.9	2.043	23730	3278.9600	0.4734	4098.7	4.0987E5	3.411E-3	0.6	1.1
37.000	183.3	1473.6	10000	20.0	5.788	67.000	480.3	229.1	2.097	23580	3430.5701	0.4494	4288.2	4.2882E5	3.411E-3	0.6	1.1
37.992	189.3	1563.2	10000	20.0	5.763	67.992	509.5	236.6	2.153	23480	3664.7400	0.4194	4580.9	4.5809E5	3.411E-3	0.6	1.1
39.100	195.5	1637.4	10000	20.0	5.744	69.100	533.7	244.4	2.183	23400	3905.6299	0.3917	4882.0	4.8820E5	3.411E-3	0.7	1.2
39.992	199.7	1726.0	10000	20.0	5.722	69.992	562.6	249.6	2.254	23310	4068.2500	0.3742	5085.3	5.0853E5	3.411E-3	0.7	1.2
41.012	203.7	1798.7	10000	20.0	5.703	71.012	586.3	254.6	2.303	23240	4232.4399	0.3585	5290.6	5.2906E5	3.411E-3	0.7	1.2
42.280	210.0	1914.4	10000	20.0	5.657	72.280	624.0	262.4	2.378	23050	4497.6001	0.3346	5622.0	5.6220E5	3.411E-3	0.7	1.2
42.992	214.1	1975.1	10000	20.0	5.619	72.992	643.8	267.6	2.406	22890	4674.1899	0.3197	5842.7	5.8427E5	3.411E-3	0.7	1.2
44.008	218.1	2063.5	10000	20.0	5.605	74.008	672.6	272.7	2.467	22840	4851.1001	0.3072	6063.9	6.0639E5	3.411E-3	0.7	1.2
45.012	224.3	2183.5	10000	20.0	5.576	75.012	711.7	280.3	2.539	22720	5128.7402	0.2891	6410.9	6.4109E5	3.411E-3	0.8	1.3
45.992	228.4	2260.2	10000	20.0	5.547	75.992	736.7	285.5	2.581	22600	5318.1602	0.2773	6647.7	6.6477E5	3.411E-3	0.8	1.3
47.012	234.5	2364.3	10000	20.0	5.514	77.012	770.6	293.1	2.629	22470	5603.0098	0.2615	7003.8	7.0038E5	3.411E-3	0.8	1.3
48.012	238.5	2440.2	10000	20.0	5.487	78.012	795.4	298.1	2.668	22360	5797.5400	0.2515	7246.9	7.2469E5	3.411E-3	0.8	1.3
49.008	242.7	2517.9	10000	20.0	5.462	79.008	820.7	303.3	2.705	22250	6000.3198	0.2418	7500.4	7.5004E5	3.411E-3	0.8	1.3
50.008	248.8	2642.2	10000	20.0	5.418	80.008	861.2	310.9	2.770	22070	6302.1802	0.2283	7877.7	7.8777E5	3.411E-3	0.8	1.3
51.012	252.8	2709.4	10000	20.0	5.399	81.012	883.1	316.0	2.795	22000	6510.3301	0.2203	8137.9	8.1379E5	3.411E-3	0.9	1.4
51.992	259.0	2853.4	10000	20.0	5.365	81.992	930.0	323.8	2.873	21860	6831.9702	0.2085	8540.0	8.5400E5	3.411E-3	0.9	1.4
52.992	263.1	2935.9	10000	20.0	5.327	82.992	956.9	328.9	2.910	21700	7047.2598	0.2007	8809.1	8.8091E5	3.411E-3	0.9	1.4
54.000	269.2	3074.9	10000	20.0	5.265	84.000	1002	336.5	2.979	21450	7374.1499	0.1895	9217.7	9.2177E5	3.411E-3	0.9	1.4
55.008	273.3	3165.8	10000	20.0	5.242	85.008	1032	341.6	3.021	21360	7604.5098	0.1831	9505.6	9.5056E5	3.411E-3	0.9	1.4
56.008	277.3	3253.2	10000	20.0	5.201	86.008	1060	346.7	3.059	21190	7828.1099	0.1763	9785.1	9.7851E5	3.411E-3	0.9	1.4
57.004	283.4	3386.1	10000	20.0	5.179	87.004	1104	354.2	3.116	21100	8168.4600	0.1682	10211	1.0211E6	3.411E-3	1.0	1.5
58.008	287.5	3471.5	10000	20.0	5.132	88.008	1132	359.3	3.149	20910	8409.5400	0.1619	10512	1.0512E6	3.411E-3	1.0	1.5
59.024	293.6	3607.8	10000	20.0	5.092	89.024	1176	367.0	3.204	20750	8767.4102	0.1541	10959	1.0959E6	3.411E-3	1.0	1.5
60.012	297.6	3717.9	10000	20.0	5.060	90.012	1212	372.0	3.258	20620	9006.9004	0.1490	11259	1.1259E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0120	300.0	3789.4	10000	20.0	5.041	92.012	1235	375.0	3.293	20540	279.5920	0.1460	349.49	34949	3.411E-3	0.0	1.5
2.0040	300.0	3808.8	10000	20.0	5.056	93.004	1241	375.0	3.311	20600	530.9580	0.1465	663.70	66370	3.411E-3	0.0	1.6
3.0040	300.0	3801.9	10000	20.0	5.056	94.004	1239	375.0	3.305	20600	907.8400	0.1465	1134.8	1.1348E5	3.411E-3	0.1	1.6
4.0000	300.0	3788.6	10000	20.0	5.037	95.000	1235	375.0	3.293	20520	1160.7700	0.1459	1451.0	1.4510E5	3.411E-3	0.1	1.6
5.0000	300.0	3811.7	10000	20.0	5.051	96.000	1242	375.0	3.313	20580	1538.0500	0.1464	1922.6	1.9226E5	3.411E-3	0.1	1.6
6.0000	300.0	3776.7	10000	20.0	5.051	97.000	1231	375.0	3.283	20580	1787.6300	0.1463	2234.5	2.2345E5	3.411E-3	0.1	1.6
7.0080	300.0	3738.1	10000	20.0	4.996	98.008	1218	375.0	3.249	20360	2038.7700	0.1448	2548.5	2.5485E5	3.411E-3	0.1	1.6
8.0000	300.0	3767.9	10000	20.0	5.054	99.000	1228	375.0	3.275	20590	2417.2800	0.1464	3021.6	3.0216E5	3.411E-3	0.1	1.7
9.0080	300.0	3767.3	10000	20.0	5.062	100.008	1228	375.0	3.275	20620	2667.0500	0.1467	3333.8	3.3338E5	3.411E-3	0.2	1.7
10.008	300.0	3772.7	10000	20.0	5.057	101.008	1230	375.0	3.279	20610	2918.4900	0.1465	3648.1	3.6481E5	3.411E-3	0.2	1.7
10.996	300.0	3760.1	10000	20.0	5.017	101.996	1226	375.0	3.268	20440	3295.5100	0.1454	4119.4	4.1194E5	3.411E-3	0.2	1.7
12.020	300.0	3759.1	10000	20.0	5.030	103.020	1225	375.0	3.267	20490	3546.9199	0.1457	4433.7	4.4337E5	3.411E-3	0.2	1.7
13.012	300.0	3765.0	10000	20.0	5.030	104.012	1227	375.0	3.272	20490	3925.0200	0.1457	4906.3	4.9063E5	3.411E-3	0.2	1.7
14.012	300.0	3771.6	10000	20.0	5.057	105.012	1229	375.0	3.278	20610	4177.4399	0.1465	5221.8	5.2218E5	3.411E-3	0.2	1.8
15.008	300.0	3798.4	10000	20.0	5.054	106.008	1238	375.0	3.301	20590	4426.3701	0.1464	5533.0	5.5330E5	3.411E-3	0.3	1.8
16.012	300.0	3804.2	10000	20.0	5.064	107.012	1240	375.0	3.307	20630	4804.9600	0.1467	6006.2	6.0062E5	3.411E-3	0.3	1.8
17.004	300.0	3776.7	10000	20.0	5.060	108.004	1231	375.0	3.283	20620	5054.6602	0.1466	6318.3	6.3183E5	3.411E-3	0.3	1.8
18.012	300.0	3790.8	10000	20.0	5.112	109.012	1236	375.0	3.295	20830	5436.2202	0.1481	6795.3	6.7953E5	3.411E-3	0.3	1.8
19.000	300.0	3782.0	10000	20.0	5.038	110.000	1233	375.0	3.287	20530	5683.1299	0.1460	7103.9	7.1039E5	3.411E-3	0.3	1.8
20.004	300.0	3798.7	10000	20.0	5.064	111.004	1238	375.0	3.302	20630	5934.8398	0.1467	7418.6	7.4186E5	3.411E-3	0.3	1.9
21.004	300.0	3786.3	10000	20.0	5.078	112.004	1234	375.0	3.291	20690	6311.3301	0.1471	7889.2	7.8892E5	3.411E-3	0.4	1.9
22.008	300.0	3768.5	10000	20.0	5.068	113.008	1228	375.0	3.275	20650	6562.7202	0.1468	8203.4	8.2034E5	3.411E-3	0.4	1.9
22.996	300.0	3768.6	10000	20.0	5.057	113.996	1228	375.0	3.276	20600	6941.1499	0.1465	8676.4	8.6764E5	3.411E-3	0.4	1.9
24.000	300.0	3755.8	10000	20.0	5.023	115.000	1224	375.0	3.264	20470	7192.2798	0.1455	8990.4	8.9904E5	3.411E-3	0.4	1.9
25.000	300.0	3743.8	10000	20.0	5.023	116.000	1220	375.0	3.254	20470	7442.3198	0.1456	9302.9	9.3029E5	3.411E-3	0.4	1.9
26.000	300.0	3766.4	10000	20.0	5.027	117.000	1228	375.0	3.274	20480	7821.4600	0.1457	9776.8	9.7768E5	3.411E-3	0.4	2.0
27.004	300.0	3756.2	10000	20.0	5.024	118.004	1224	375.0	3.265	20470	8070.7202	0.1456	10088	1.0088E6	3.411E-3	0.5	2.0
28.000	300.0	3771.9	10000	20.0	5.038	119.000	1229	375.0	3.279	20530	8324.1602	0.1460	10405	1.0405E6	3.411E-3	0.5	2.0
29.000	300.0	3770.7	10000	20.0	5.014	120.000	1229	375.0	3.277	20430	8698.9697	0.1453	10874	1.0874E6	3.411E-3	0.5	2.0
29.996	300.0	3782.2	10000	20.0	5.074	120.996	1233	375.0	3.287	20670	8950.3203	0.1470	11188	1.1188E6	3.411E-3	0.5	2.0
31.000	300.0	3778.6	10000	20.0	5.057	122.000	1232	375.0	3.284	20600	9327.2305	0.1465	11659	1.1659E6	3.411E-3	0.5	2.0
31.996	300.0	3805.0	10000	20.0	5.054	122.996	1240	375.0	3.307	20590	9579.0898	0.1464	11974	1.1974E6	3.411E-3	0.5	2.0
33.000	300.0	3771.7	10000	20.0	5.052	124.000	1229	375.0	3.278	20580	9830.6504	0.1464	12288	1.2288E6	3.411E-3	0.6	2.1
34.000	300.0	3726.4	10000	20.0	5.080	125.000	1215	375.1	3.238	20700	10208.600	0.1472	12761	1.2761E6	3.411E-3	0.6	2.1
35.000	300.0	3783.3	10000	20.0	5.042	126.000	1233	374.9	3.289	20540	10460.000	0.1461	13075	1.3075E6	3.411E-3	0.6	2.1
35.996	300.0	3777.4	10000	20.0	5.056	126.996	1231	375.0	3.283	20600	10838.000	0.1465	13548	1.3548E6	3.411E-3	0.6	2.1
37.004	300.0	3753.1	10000	20.0	5.023	128.004	1223	375.0	3.262	20470	11091.300	0.1455	13864	1.3864E6	3.411E-3	0.6	2.1
38.000	300.0	3783.5	10000	20.0	5.053	129.000	1233	375.0	3.289	20590	11338.200	0.1464	14173	1.4173E6	3.411E-3	0.6	2.2
39.000	300.0	3764.2	10000	20.0	5.061	130.000	1227	375.0	3.272	20620	11717.300	0.1466	14647	1.4647E6	3.411E-3	0.7	2.2
40.048	300.0	3768.9	10000	20.0	5.043	131.048	1228	375.0	3.276	20550	11967.000	0.1461	14959	1.4959E6	3.411E-3	0.7	2.2
40.996	300.0	3760.3	10000	20.0	5.037	131.996	1226	375.0	3.268	20520	12217.700	0.1459	15272	1.5272E6	3.411E-3	0.7	2.2
42.004	300.0	3757.6	10000	20.0	5.039	133.004	1225	375.0	3.266	20530	12594.800	0.1460	15744	1.5744E6	3.411E-3	0.7	2.2
43.000	300.0	3765.2	10000	20.0	5.053	134.000	1227	375.0	3.273	20590	12845.900	0.1464	16057	1.6057E6	3.411E-3	0.7	2.2
43.996	300.0	3805.5	10000	20.0	5.091	134.996	1240	375.0	3.308	20740	13223.000	0.1475	16529	1.6529E6	3.411E-3	0.7	2.2
45.000	300.0	3797.4	10000	20.0	5.095	136.000	1238	375.0	3.301	20760	13474.100	0.1476	16843	1.6843E6	3.411E-3	0.8	2.3
45.996	300.0	3814.9	10000	20.0	5.036	136.996	1243	375.0	3.316	20520	13725.600	0.1459	17157	1.7157E6	3.411E-3	0.8	2.3
47.004	300.0	3819.0	10000	20.0	5.071	138.004	1245	375.0	3.319	20660	14102.500	0.1469	17628	1.7628E6	3.411E-3	0.8	2.3
48.000	300.0	3800.2	10000	20.0	5.025	139.000	1239	375.0	3.303	20470	14353.800	0.1456	17942	1.7942E6	3.411E-3	0.8	2.3
48.996	300.0	3793.1	10000	20.0	5.063	139.996	1236	375.0	3.297	20630	14731.100	0.1467	18414	1.8414E6	3.411E-3	0.8	2.3
50.000	300.0	3805.8	10000	20.0	5.072	141.000	1241	375.0	3.308	20670	14982.100	0.1469	18728	1.8728E6	3.411E-3	0.8	2.4
51.000	300.0	3794.4	10000	20.0	5.071	142.000	1237	375.0	3.298	20660	15233.500	0.1469	19042	1.9042E6	3.411E-3	0.9	2.4
52.004	300.0	3794.2	10000	20.0	5.065	143.004	1237	375.0	3.298	20640	15610.500	0.1468	19513	1.9513E6	3.411E-3	0.9	2.4
53.000	300.0	3798.6	10000	20.0	5.038	144.000	1238	375.0	3.301	20530	15861.800	0.1459	19827	1.9827E6	3.411E-3	0.9	2.4
54.000	300.0	3819.5	10000	20.0	5.011	145.000	1245	375.0	3.320	20420	16243.700	0.1452	20305	2.0305E6	3.411E-3	0.9	2.4
55.000	300.0	3783.8	10000	20.0	5.051	146.000	1233	375.0	3.289	20580	16490.199	0.1463	20613	2.0613E6	3.411E-3	0.9	2.4
55.996	300.0	3767.9	10000	20.0	5.073	146.996	1228	375.0	3.275	20670	16747.900	0.1470	20935	2.0935E6	3.411E-3	0.9	2.4
57.004	300.0	3771.3	10000	20.0	5.041	148.004	1229	375.0	3.278	20540	17118.500	0.1461	21398	2.1398E6	3.411E-3	1.0	2.5
58.000	300.0	3766.5	10000	20.0	5.028	149.000	1228	375.0	3.274	20490	17370.699	0.1457	21713	2.1713E6	3.411E-3	1.0	2.5
59.000	300.0	3799.4	10000	20.0	5.049	150.000	1238	375.0	3.303	20570	17621.199	0.1463	22027	2.2027E6	3.411E-3	1.0	2.5
60.000	300.0	3761.5	10000	20.0	5.052	151.000	1226	375.0	3.270	20580	17998.699	0.1464	22498	2.2498E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0280	296.2	3711.4	10000	20.0	5.095	152.028	1210	370.2	3.268	20760	322.1440	0.1515	402.68	40268	3.411E-3	0.0	2.5
2.0440	292.1	3599.7	10000	20.0	5.087	153.044	1173	365.2	3.213	20730	561.2520	0.1554	701.57	70157	3.411E-3	0.0	2.6
3.0440	286.0	3493.6	10000	20.0	5.175	154.044	1139	357.5	3.185	21090	916.0420	0.1650	1145.1	1.1451E5	3.411E-3	0.1	2.6
4.0440	281.9	3335.8	10000	20.0	5.201	155.044	1087	352.4	3.085	21190	1153.9800	0.1706	1442.5	1.4425E5	3.411E-3	0.1	2.6
5.1440	275.8	3215.1	10000	20.0	5.245	156.144	1048	344.8	3.039	21370	1492.2300	0.1797	1865.3	1.8653E5	3.411E-3	0.1	2.6
6.0440	271.8	3136.6	10000	20.0	5.251	157.044	1022	339.7	3.010	21390	1719.4900	0.1854	2149.4	2.1494E5	3.411E-3	0.1	2.6
7.1000	267.6	3030.1	10000	20.0	5.290	158.100	987.7	334.5	2.952	21550	1942.8900	0.1926	2428.6	2.4286E5	3.411E-3	0.1	2.6
8.0280	261.6	2924.2	10000	20.0	5.343	159.028	953.1	327.0	2.915	21770	2264.0901	0.2036	2830.1	2.8301E5	3.411E-3	0.1	2.7
9.0520	257.5	2841.1	10000	20.0	5.391	160.052	926.0	321.9	2.877	21970	2476.1499	0.2120	3095.2	3.0952E5	3.411E-3	0.2	2.7
10.044	251.3	2761.8	10000	20.0	5.399	161.044	900.2	314.2	2.865	22000	2799.5300	0.2228	3499.4	3.4994E5	3.411E-3	0.2	2.7
11.048	247.3	2653.4	10000	20.0	5.424	162.048	864.9	309.1	2.798	22100	2996.7600	0.2314	3746.0	3.7460E5	3.411E-3	0.2	2.7
12.060	243.2	2540.6	10000	20.0	5.457	163.060	828.1	304.1	2.724	22230	3195.1201	0.2405	3993.9	3.9939E5	3.411E-3	0.2	2.7
13.048	237.1	2423.1	10000	20.0	5.489	164.048	789.8	296.3	2.665	22370	3495.4900	0.2547	4369.4	4.3694E5	3.411E-3	0.2	2.7
14.044	232.9	2348.2	10000	20.0	5.524	165.044	765.4	291.1	2.629	22510	3689.3201	0.2656	4611.7	4.6117E5	3.411E-3	0.2	2.8
15.044	226.8	2241.6	10000	20.0	5.549	166.044	730.6	283.5	2.577	22610	3978.5300	0.2813	4973.2	4.9732E5	3.411E-3	0.3	2.8
16.060	222.7	2173.9	10000	20.0	5.570	167.060	708.6	278.4	2.546	22690	4158.6602	0.2929	5198.3	5.1983E5	3.411E-3	0.3	2.8
17.044	218.6	2082.7	10000	20.0	5.601	168.044	678.8	273.2	2.485	22820	4428.7402	0.3058	5535.9	5.5359E5	3.411E-3	0.3	2.8
18.048	212.5	1982.3	10000	20.0	5.629	169.048	646.1	265.6	2.432	22930	4602.8799	0.3250	5753.6	5.7536E5	3.411E-3	0.3	2.8
19.044	208.4	1892.9	10000	20.0	5.663	170.044	617.0	260.5	2.368	23070	4777.8599	0.3400	5972.3	5.9723E5	3.411E-3	0.3	2.8
20.044	202.1	1798.3	10000	20.0	5.691	171.044	586.1	252.7	2.320	23190	5034.3799	0.3632	6293.0	6.2930E5	3.411E-3	0.3	2.9
21.044	198.1	1719.9	10000	20.0	5.723	172.044	560.6	247.6	2.264	23320	5196.9302	0.3803	6496.2	6.4962E5	3.411E-3	0.4	2.9
22.044	191.9	1646.4	10000	20.0	5.734	173.044	536.6	239.9	2.237	23360	5441.9102	0.4059	6802.4	6.8024E5	3.411E-3	0.4	2.9
23.044	187.7	1544.7	10000	20.0	5.766	174.044	503.5	234.6	2.146	23490	5603.2402	0.4268	7004.1	7.0041E5	3.411E-3	0.4	2.9
24.044	183.6	1488.8	10000	20.0	5.783	175.044	485.3	229.5	2.115	23560	5754.1899	0.4474	7192.7	7.1927E5	3.411E-3	0.4	2.9
25.044	177.4	1378.3	10000	20.0	5.805	176.044	449.3	221.8	2.026	23650	5978.9702	0.4808	7473.7	7.4737E5	3.411E-3	0.4	2.9
26.044	173.2	1325.3	10000	20.0	5.840	177.044	432.0	216.5	1.996	23790	6128.3398	0.5078	7660.4	7.6604E5	3.411E-3	0.4	3.0
27.044	169.1	1255.6	10000	20.0	5.853	178.044	409.3	211.4	1.936	23850	6336.3301	0.5336	7920.4	7.9204E5	3.411E-3	0.5	3.0
28.044	163.0	1171.6	10000	20.0	5.879	179.044	381.9	203.7	1.875	23950	6477.6499	0.5772	8097.1	8.0971E5	3.411E-3	0.5	3.0
29.044	158.8	1106.2	10000	20.0	5.885	180.044	360.6	198.4	1.817	23980	6610.1001	0.6089	8262.6	8.2626E5	3.411E-3	0.5	3.0
30.048	152.5	1024.2	10000	20.0	5.919	181.048	333.9	190.6	1.752	24120	6803.2202	0.6639	8504.0	8.5040E5	3.411E-3	0.5	3.0
31.044	148.4	960.40	10000	20.0	5.932	182.044	313.0	185.5	1.688	24170	6928.7300	0.7026	8660.9	8.6609E5	3.411E-3	0.5	3.0
32.044	144.1	912.88	10000	20.0	5.952	183.044	297.6	180.2	1.651	24250	7052.7402	0.7470	8815.9	8.8159E5	3.411E-3	0.5	3.1
33.044	137.9	819.94	10000	20.0	5.982	184.044	267.3	172.4	1.550	24370	7227.4502	0.8203	9034.3	9.0343E5	3.411E-3	0.6	3.1
34.028	133.8	777.60	10000	20.0	5.992	185.028	253.5	167.3	1.515	24420	7339.7202	0.8727	9174.7	9.1747E5	3.411E-3	0.6	3.1
35.040	129.6	732.66	10000	20.0	6.001	186.040	238.8	162.0	1.474	24450	7451.9302	0.9319	9314.9	9.3149E5	3.411E-3	0.6	3.1
36.044	123.1	667.40	10000	20.0	6.022	187.044	217.5	153.9	1.414	24540	7616.0098	1.036	9520.0	9.5200E5	3.411E-3	0.6	3.1
37.044	119.0	629.89	10000	20.0	6.032	188.044	205.3	148.8	1.380	24570	7714.5498	1.110	9643.2	9.6432E5	3.411E-3	0.6	3.1
38.044	114.8	590.63	10000	20.0	6.035	189.044	192.5	143.5	1.341	24590	7813.5698	1.194	9767.0	9.7670E5	3.411E-3	0.6	3.2
39.044	108.3	530.83	10000	20.0	6.050	190.044	173.0	135.4	1.278	24650	7956.7500	1.345	9945.9	9.9459E5	3.411E-3	0.7	3.2
40.044	104.3	498.44	10000	20.0	6.063	191.044	162.5	130.3	1.247	24700	8044.8101	1.454	10056	1.0056E6	3.411E-3	0.7	3.2
41.044	100.0	459.39	10000	20.0	6.071	192.044	149.7	125.0	1.198	24730	8175.3301	1.582	10219	1.0219E6	3.411E-3	0.7	3.2
42.048	93.35	408.89	10000	20.0	6.081	193.048	133.3	116.7	1.142	24770	8261.5195	1.820	10327	1.0327E6	3.411E-3	0.7	3.2
43.040	89.13	375.26	10000	20.0	6.083	194.040	122.3	111.4	1.098	24790	8336.4102	1.997	10421	1.0421E6	3.411E-3	0.7	3.2
44.044	84.89	344.14	10000	20.0	6.087	195.044	112.2	106.1	1.057	24800	8410.6504	2.202	10513	1.0513E6	3.411E-3	0.7	3.3
45.044	80.43	313.28	10000	20.0	6.096	196.044	102.1	100.5	1.016	24840	8485.0195	2.457	10606	1.0606E6	3.411E-3	0.8	3.3
46.044	73.87	268.92	10000	20.0	6.106	197.044	87.65	92.34	0.9493	24880	8584.2402	2.918	10730	1.0730E6	3.411E-3	0.8	3.3
47.044	69.58	249.61	10000	20.0	6.113	198.044	81.36	86.97	0.9355	24910	8646.3203	3.292	10808	1.0808E6	3.411E-3	0.8	3.3
48.044	65.04	216.24	10000	20.0	6.117	199.044	70.48	81.29	0.8670	24920	8707.9600	3.771	10885	1.0885E6	3.411E-3	0.8	3.3
49.040	58.34	186.98	10000	20.0	6.128	200.040	60.95	72.92	0.8357	24970	8788.4902	4.695	10986	1.0986E6	3.411E-3	0.8	3.3
50.044	53.99	160.21	10000	20.0	6.132	201.044	52.22	67.49	0.7738	24990	8837.5703	5.486	11047	1.1047E6	3.411E-3	0.8	3.4
51.040	49.27	137.19	10000	20.0	6.134	202.040	44.72	61.58	0.7261	24990	8886.6904	6.590	11108	1.1108E6	3.411E-3	0.9	3.4
52.040	44.41	116.65	10000	20.0	6.140	203.040	38.02	55.51	0.6849	25020	8929.6299	8.117	11162	1.1162E6	3.411E-3	0.9	3.4
53.044	40.10	96.137	10000	20.0	6.142	204.044	31.34	50.12	0.6252	25020	8966.5098	9.960	11208	1.1208E6	3.411E-3	0.9	3.4
54.040	35.28	79.351	10000	20.0	6.148	205.040	25.86	44.10	0.5865	25050	9003.0596	12.88	11254	1.1254E6	3.411E-3	0.9	3.4
55.044	30.24	60.342	10000	20.0	6.149	206.044	19.67	37.80	0.5203	25050	9034.6699	17.54	11293	1.1293E6	3.411E-3	0.9	3.4
56.044	25.93	46.664	10000	20.0	6.154	207.044	15.21	32.42	0.4692	25070	9057.5498	23.86	11322	1.1322E6	3.411E-3	0.9	3.5
57.036	20.85	33.066	10000	20.0	6.153	208.036	10.78	26.07	0.4135	25070	9081.3301	36.90	11352	1.1352E6	3.411E-3	1.0	3.5
58.040	17.84	25.573	10000	20.0	6.155	209.040	8.336	22.30	0.3738	25080	9092.8799	50.42	11366	1.1366E6	3.411E-3	1.0	3.5
59.028	11.12	11.121	10000	20.0	6.158	210.028	3.625	13.90	0.2608	25090	9109.6504	129.9	11387	1.1387E6	3.411E-3	1.0	3.5
60.040	5.494	2.1851	10000	20.0	6.155	211.040	0.7122	6.867	0.1037	25080	9117.5303	531.8	11397	1.1397E6	3.411E-3	1.0	3.5

